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Beilstein J. Org. Chem. 2019, 15, 710–720, doi:10.3762/bjoc.15.66
Graphical Abstract
Figure 1: Schematic representation of β-CD with glucopyranose atom numbering and with alphabetic labeling of ...
Scheme 1: Syntheses of 6A,6X-diazido-β-CDs as reference compounds using the “capping” literature method [11,12].
Scheme 2: Syntheses of homo-difunctionalized β-CDs using different reaction conditions.
Figure 2: HPLC chromatograms of the authentic 6A,6X-diazido-β-CDs with known regiochemistry (references 1–3, Scheme 1...
Figure 3: NMR spectral regions of the three ditosyl regioisomers in D2O (500 MHz). The signals of the tosylat...
Scheme 3: Syntheses of 6A-monoazido-6X-monotosyl-β-CDs using starting materials obtained from different react...
Figure 4: Reversed-phase HPLC chromatograms of 6A-monoazido-6X-monotosyl-β-CDs prepared through reactions 4–8....
Figure 5: HPLC separation of regioisomers and pseudoenantiomers of 6A-monoazido-6X-monotosyl-β-CD prepared in...
Figure 6: Reversed-phase HPLC chromatograms of 6A,6X-diazido-β-CDs prepared in reactions 9–13.
Beilstein J. Org. Chem. 2016, 12, 2873–2882, doi:10.3762/bjoc.12.286
Figure 1: Adsorption of β-CD on the surface of nanoTiO2 [37].
Figure 2: Turbidity of nanoTiO2 dispersion (0.02%) in the presence of 1% HPBCD-P (green diamond) and 1% CMBCD...
Figure 3: Aggregation effect of 0.1% NaCl on 0.02% nanoTiO2 dispersion in the absence (green curve) and prese...
Figure 4: Aggregation effect of tap water on 0.02% nanoTiO2 dispersion in the absence (green curve) and prese...
Figure 5: Photodegradation of MB in aqueous solutions: distilled water (A), 0.1% NaCl solution (B) and tap wa...
Figure 6: Photodegradation of IBR in distilled water examining the drug itself (blue circle), and in the pres...